The CRM is available in a glass vial containing 32 g of cryo-milled soya bean powder in an atmosphere of dry nitrogen. A variety of extraction and purification methods were used in combination with liquid and/or gas chromatography coupled to tandem mass spectrometry or gas chromatography coupled to electron capture detection (ECD).
Inhalte
Analyt
CAS-Nummer
Konzentration
Einheit
Zusätzliche Informationen
Methode
Azoxystrobin
[131860-33-8]
0,46 ± 0,05
mg/kg
Certified value
Carbendazim
[10605-21-7]
0,197 ± 0,019
mg/kg
Certified value
As obtained by liquid chromatography/tandem mass spectrometry
Chlorpyrifos
[2921-88-2]
0,067 ± 0,006
mg/kg
Certified value
Cypermethrin
[52315-07-8]
0,052 ± 0,01
mg/kg
Certified value
Diazinon
[333-41-5]
0,068 ± 0,006
mg/kg
Certified value
Dieldrin
[60-57-1]
0,075 ± 0,007
mg/kg
Certified value
As obtained by gas chromatography
Endosulfan (alpha and beta)
[115-29-7]
0,49 ± 0,05
mg/kg
Certified value
As obtained by gas chromatography
Imidacloprid
[138261-41-3]
0,075 ± 0,009
mg/kg
Certified value
As obtained by liquid chromatography/tandem mass spectrometry
Iprodione
[36734-19-7]
0,104 ± 0,015
mg/kg
Certified value
Methomyl
[16752-77-5]
0,046 ± 0,006
mg/kg
Certified value
As obtained by liquid chromatography/tandem mass spectrometry
Tebuconazole
[107534-96-3]
0,048 ± 0,005
mg/kg
Certified value
Endosulfan-I (alpha)
[959-98-8]
0,08 - 0,15
mg/kg
Additional material information
Endosulfan-II (beta)
[33213-65-9]
0,28 - 0,47
mg/kg
Additional material information
AnalytCarbendazimCAS-Nummer[10605-21-7]Konzentration0,197 ± 0,019Einheitmg/kgZusätzliche InformationenCertified valueMethodeAs obtained by liquid chromatography/tandem mass spectrometry
AnalytDieldrinCAS-Nummer[60-57-1]Konzentration0,075 ± 0,007Einheitmg/kgZusätzliche InformationenCertified valueMethodeAs obtained by gas chromatography
AnalytEndosulfan (alpha and beta)CAS-Nummer[115-29-7]Konzentration0,49 ± 0,05Einheitmg/kgZusätzliche InformationenCertified valueMethodeAs obtained by gas chromatography
AnalytImidaclopridCAS-Nummer[138261-41-3]Konzentration0,075 ± 0,009Einheitmg/kgZusätzliche InformationenCertified valueMethodeAs obtained by liquid chromatography/tandem mass spectrometry